Download Inorganic Syntheses, Volume 8 by Henry F. Holtzclaw, Volume 8 PDF

By Henry F. Holtzclaw, Volume 8

The volumes during this carrying on with sequence offer a compilation of present innovations and ideas in inorganic man made chemistry. contains inorganic polymer syntheses and education of significant inorganic solids, syntheses utilized in the advance of pharmacologically energetic inorganic compounds, small-molecule coordination complexes, and similar compounds. additionally includes priceless info on transition organometallic compounds together with species with metal-metal cluster molecules. All syntheses provided right here were validated.

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76, 793 (1963). 9. C. K R ~ Q Eand R E. G. ROCHOW: J . Organometal. , 1,476 (1964). 6. LITHIUM BIS(TR1METHYLSILYL)AMIDE AND TRIS (TRIMETHYLSILYL)AMINE SUBMITTED BY E. H. AMONOO-NEIZER, * R. A. SHAW, * D. 0. SHOVLIN, * and B. C. SMITH* CHECKED B Y JOELw. ROSENTHAL? AND WILLIAM L. JoLLYt Ammonia reacts with trimethylchlorosilane to give hexamethyldisilaaane, but tris(trimethylsily1)amine is not formed by this reaction. Hexamethyldisilazane reacts with n-butyllithium to give lithium bis(trimethylsily1)amide, which is a strong nucleophilic reagent.

REYNOLDS: J. Chem. , 89, 397 (1906). G. S. FORBES and H. H. ANDERSON: J . Am. Chem. ,67,1911 (1945). H. H. , 69, 3049 (1947). H. H. , 72, 193 (1950). H. H. , 72, 196 (1950). H. , 72, 2761 (1950). H. H. , 76, 1576 (1953). J. J. MCBRIDEand H. C. , 74, 5247 (1952). M. G. VORONKOV and B. N. D o ~ c o v“Soviet : Research in Organo-Silicon Chemistry, 1949-56,” English Translation, Part 11, pp. , New York. 12. R. G. NEVILLEand J. J. MCGEE:Org. Syntheses, 46, 69 (1965). 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11.

10. 11. 8. A. HOOTON* c. KoTZt A N D A. LA U BEN C A Y ER t CHECKED BY JOHN - A. 2 Complete removal of excess magnesium is essential to avoid the formation of hexaphenyldigermane as a by-product. Procedure Phenylmagnesium bromide solution [resulting from the reaction of 88 g. 6 g. * The University of Durham, Durham City, England. Y. Inorganic Syntheses, Volume VIII Edited by Henry F. Holtzclaw, Jr. Copyright © 1966 by McGraw-Hill Book Company, Inc. T E T RAPHEN YLGERMAN E 31 References P. MIQUEL:BuU.

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